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54477 1969-12-31 [Biofuel] Seperating glycerine	54505 1969-12-31 [Biofuel] seperating Glycerine
54535 2005-12-01 Re: [Biofuel] seperating Glycerine..	54547 2005-12-02 Re: [Biofuel] seperating Glycerine..

Message #54505 of 54591
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Date: 2005-12-02
From: john owens
Subject: [Biofuel] seperating Glycerine

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Hi,

I did couple of tests on glycerin separation with the titration method
on JTF with different results.

Test One;
250ml byproduct
10ml phosphoric
shacked vigorously

There was separation with 3 layers about 60/30/10 within about 15 minutes.
FFa Glycerin and fluffy white sodium phosphate

Test two;
250ml byproduct
10ml phosphoric
shaked vigorously
I then added 5ml phosphoric
shaked vigorously
I added  more phosphoric  to see what would happen.

there was separation with In about one minute with two layers about 50/50
with creamy brown stuff on the bottom. FFa on top

I then added more phosphoric until I got separation of a reddish colour
onbottom. this has being sitting for 4 hours or so.
In the jar there is about *(40/60 (ffa/glycerin)* with a very fine white
layer on the bottom.

I made a mistake with the last mail.

There is a greater amount of glycerin in test two and less ffa

Could any one explain to me what is happening

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Hi,

I did couple of tests on glycerin separation with the titra=
tion method
on JTF with different results.

Test One;
250ml byp=
roduct
10ml phosphoric
shacked vigorously

There was separation=
 with 3 layers about 60/30/10 within about 15 minutes.

FFa Glycerin and fluffy white sodium phosphate

Test two;
250m=
l byproduct
10ml phosphoric
shaked vigorously
I then added 5ml pho=
sphoric
shaked vigorously
I added  more phosphoric  to see =
what would happen.


there was separation with In about one minute with two layers about=
 50/50
with creamy brown stuff on the bottom. FFa on top

I then a=
dded more phosphoric until I got separation of a reddish colour onbottom. t=
his has being sitting for 4 hours or so.

In the jar there is about (40/60 (ffa/glycerin)=
 with a very fine white layer on the bottom.   
           &nbs=
p;            &=
nbsp;           &nbs=
p;    
I made a mistake with the last mail.

There is a greater amount =
of glycerin in test two and less ffa

Could any one explain to me wha=
t is happening

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